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Журнал аналитической химии, 2023, T. 78, № 10, стр. 897-913

Атомно-спектральные методы в исследовании свойств и поведения наноразмерных магнитных материалов в биологических системах

И. В. Кубракова a, *, О. Н. Гребнева-Балюк a, Д. В. Пряжников a, М. С. Киселева a, О. О. Ефанова a

a Институт геохимии и аналитической химии им. В.И. Вернадского Российской академии наук
119991 Москва, ул. Косыгина, 19, Россия

* E-mail: kubrakova@geokhi.ru

Поступила в редакцию 03.04.2023
После доработки 17.05.2023
Принята к публикации 17.05.2023

Аннотация

Кратко рассмотрены способы получения и некоторые виды магнитных наночастиц (МНЧ), перспективных для биомедицинских исследований. Показана связь строения и свойств частиц с областями их применения в медицинской диагностике и биоанализе. Особое внимание уделено МНЧ, содержащим благородные металлы в качестве биомаркеров или действующего вещества. Рассмотрены биомедицинские задачи, реализуемые с помощью МНЧ, и аналитические пути их решения. Обобщены данные о применении прямых и комбинированных атомно-спектральных (ЭТААС, АЭС/МС-ИСП) методов в биомедицинских исследованиях. Рассмотрены экспериментальные подходы к изучению поведения и превращений МНЧ in vitro и in vivo. Подчеркнута ключевая роль пробоподготовки в экспериментальном моделировании поведения НЧ в биологических средах. Отмечены особенности подготовки при определении растворенных и наноразмерных форм в биообъектах. Оценены перспективы комплексных исследований поведения МНЧ в сложных биологических системах.

Ключевые слова: наноразмерные магнитные материалы, биомедицинские исследования, электротермическая атомно-абсорбционная спектрометрия (ЭТААС), масс-спектрометрия с индуктивно связанной плазмой (МС-ИСП) в режимах высокого разрешения, детектирования одиночных частиц (SP-ICP-MS) или анализа отдельных клеток (SC-ICP-MS).

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